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2014, Vol.43, No.6

799-801

Sequential Paired Electrosynthesis of a Diaryl Ether Derivative Using an Electrochemical Microreactor

Tsuneo Kashiwagi 1 , Toshio Fuchigami 1 , Tsuyoshi Saito 3 , Shigeru Nishiyama 2 , Mahito Atobe 1 , 4
1 Department of Electronic Chemistry, Tokyo Institute of Technology
2 Department of Chemistry, Faculty of Science Technology, Keio University
3 International Institute for Integrative Sleep Medicine, Tsukuba University
4 Department of Environment and System Sciences, Yokohama National University
https://doi.org/10.1246/cl.140046

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Abstract
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A paired electrosynthetic conversion of a phenol to a diaryl ether derivative by using an electrochemical microreactor has been demonstrated. Sequential anodic C–O coupling reaction of phenol 1 to dienone aryl ether 2 and following reduction of 2 took place to give diaryl ether derivative 3 selectively by simply passing an electrolytic solution through the electrochemical microreactor.

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