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2021, Vol.50, No.10

1770-1772

Hydrogen-bonding-induced Layered Assembly of Cage Siloxanes Modified with Diisopropylsilanol Groups

Naoto Sato ,1Yoshiyuki Kuroda ,2,†,‡Hiroaki Wada ,1Atsushi Shimojima ,*1,3 and Kazuyuki Kuroda *1,3
1Department of Applied Chemistry, Faculty of Science and Engineering, Waseda University, 3-4-1 Okubo, Shinjuku-ku, Tokyo 169-8555, Japan
2Waseda Institute for Advanced Study, Waseda University, 1-6-1 Nishiwaseda, Shinjuku-ku, Tokyo 169-8050, Japan
3Kagami Memorial Research Institute for Materials Science and Technology, Waseda University, 2-8-26 Nishiwaseda, Shinjuku-ku, Tokyo 169-0051, Japan
https://doi.org/10.1246/cl.210387

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Abstract

Cage siloxanes modified with diisopropylsilanol groups were synthesized and crystallized into a layered structure containing 1,3,5-trimethylbenzene molecules in the interlayer voids, which indicates that the organic groups attached to the silanol groups have an important role in the assembling behavior of cage siloxanes.

figure

Cage siloxanes modified with diisopropylsilanol groups were synthesized and crystallized into a layered structure containing 1,3,5-trimethylbenzene molecules in the interlayer voids, which indicates that the organic groups attached to the silanol groups have an important role in the assembling behavior of cage siloxanes.

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